The invention relates to a pyridone-cont...
In this article, a robust and scalable p...
The invention relates to the technical f...
The invention relates to a sulfur-contai...
2-((2,2-dimethoxyethoxy)ethyl)isoindole-1,3-dione
2-(2-aminoethoxy)-1,1-dimethoxyethane
Conditions | Yield |
---|---|
With
hydrazine hydrate; water;
In
ethanol;
at 60 ℃;
for 1h;
|
85% |
With
hydrazine hydrate;
In
ethanol; water;
at 60 ℃;
for 4h;
|
15 g |
With
hydrazine hydrate;
In
ethanol; water;
at 60 ℃;
for 4h;
|
|
With
hydrazine hydrate;
In
ethanol; water;
at 60 ℃;
for 4h;
|
2-(2-azidoethoxy)-1,1-dimethoxyethane
2-(2-aminoethoxy)-1,1-dimethoxyethane
Conditions | Yield |
---|---|
With
palladium on activated charcoal; hydrogen;
In
ethyl acetate;
at 20 ℃;
Autoclave;
|
98.1% |
With
5%-palladium/activated carbon; hydrogen;
In
methanol;
at 20 ℃;
for 24h;
Solvent;
Large scale;
|
chloroacetaldehyde dimethyl acetal
ethanolamine
2-(2,2-dimethoxyethoxy)ethyl methanesulfonate